Tailoring the crystal growth of quartz on silicon for …

This coincides with the threshold concentration range above which dense films can be stabilized over the porous morphologies, ... Curves obtained for α-quartz films with R Sr = 0.05 and R Sr = 0.033 showing their piezoelectric response (c). The graphs were obtained by averaging 4 × 4 matrix volume spectroscopy experiments in an area of …

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Combination of an electrodeless quartz crystal microbalance …

In this work, the combination of an electrodeless quartz crystal microbalance (EL-QCM) and spectrometric techniques was designed to investigate the adsorption kinetics of iodine onto two metal-organic frameworks film, MIL-101 and ZIF-67. The concentrations of I 2 adsorbed on film and in vapor phase were monitored …

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Metal-Induced Crystallization in Metal Oxides

There are other methods to micropattern quartz surfaces, and of these, the thinnest quartz crystals are about 10 μm. 49 However, when a patterned silica film is crystallized using MIC, α-quartz films as thin as 200 nm are possible, allowing the operating frequency of the material to be 50 times higher than previously fabricated …

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A novel chemical sensor using CH3Si(OCH3)3 sol-gel thin film …

Transient response curves for aromas from ethanol solutions or several kinds of alcohols with different ethanol concentrations are observed using CH 3 Si(OCH 3) 3 a sol-gel-film-coated quartz crystal resonator gas sensor. The pattern recognition analysis using principal component analysis or neural network analysis is carried out using three …

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Sputtered titania borosilicate glass films

The subsequent SIMS profiles in the quartz films confirmed that copper, silver and chromium concentrations were reduced by approximately half by suitably masking the chamber furniture. Aluminum contamination remained high, however, and may be attributable to the aluminum cathode support plate at the bottom of the chamber. The …

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Effect of growth interruption on the crystalline quality and …

Ga-doped ZnO(GZO) thin films were deposited on the quartz substrate by magnetron sputtering system with growth interruption technique. As the number of interruptions and interruption time increased, the carrier concentration and Hall mobility in GZO films significantly increased. As a result, the resistivity of GZO films decreased.

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Highly transparent and lower resistivity of yttrium doped …

We prepared YZO thin films on quartz glass substrates with respect to Y dopant concentration (Y: ... The increasing bandgap and carrier concentration of YZO thin films were interpreted by the BM shift, that is, the Fermi level moves towards the conduction band edge. The current-voltage characteristics of the heterojunction diode, …

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Electrochemical Quartz Crystal Microbalance

The electrochemical quartz crystal microbalance is a versatile technique for studying several aspects of electroactive polymer film dynamics. For rigid films, it is a sensitive probe of mobile species (ion and solvent) population changes within the film in response to redox switching. For non-rigid films, it can be used to determine film shear ...

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High Detectivity of PbS Films Deposited on Quartz …

2. Experimental Section. PbS films were grown on quartz substrates by the CBD method. The reaction solution was composed of lead acetate [Pb(CH 3 COO) 2 · 3H 2 O], trisodium citrate (C 6 H 5 Na 3 O 7), potassium hydroxide (KOH), and thiourea (CH 4 N 2 S) at a concentration ratio of 1:2:5.7:2. The cleaned quartz substrates were immersed in the …

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Investigation of thin films formed from liposome suspensions on quartz

When the concentration of unilamellar DMPC vesicles in the aqueous saline solutions was increased to 10 −1 mg/ml and stable films were formed on quartz, the dependence of the logarithm of film thickness on the time of thinning was also linear after the first 1 s for h<500 nm, as illustrated in Fig. 5.An equilibrium film thickness was …

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1-Butyl-3-Methylimidazolium Tetrafluoroborate Film as a …

9 MHz AT-cut quartz crystals (Chen Jing Electronics, Beijing, China) were used as the QCM sensor in this work. The diameter of the quartz crystal was 12.5 mm, and the gold electrode diameter was 6.0 mm. The quartz crystal was fixed to a glass tube using silicone rubber, and only one side of the crystal was coated with film for sensing.

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In-depth study on the good resistance to coke

This may be due to the fact that the composite zeolites had the lowest strong acids concentration and therefore the coke precursors were not able to generate heavy coke. This also indirectly proved that ZS-F had good regeneration performance. ... Effect of different SAPO-34 film thickness on coke resistance performance of SAPO-34/ZSM …

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Wettability of quartz by methanol and ethanol aqueous …

CONCLUSION Since tor the given alcohol concentrations in water the values of the measured contact angles lie between 6. .,, and Q-yti ^ y be concluded that the adsorption of methanoi and ethanol molecules from solution on quartz Is considerably smaller than at a solution- air interface, and that the alcohol concentration at the …

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A practical guide to quartz crystal microbalance …

Quartz crystal microbalance with dissipation (QCM‐D) monitoring is a powerful tool used to sensitively examine the real‐time responses of polymer films to external responses.

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Yttrium oxide film for protecting quartz glass surface from …

The anticorrosive property of yttrium oxide was evaluated using chlorine trifluoride gas. After the exposure to chlorine trifluoride gas at room temperature for the total time longer than 1000 min, the yttrium oxide film, formed on a quartz glass surface, did not show any etching behavior and surface morphology change, while the non-coated …

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Comparison study of V-doped ZnO thin films on polycarbonate and quartz

Vanadium (V) doped ZnO (VZO) thin films were deposited on flexible polymer and quartz substrates by RF magnetron sputtering, and influences of deposition parameters of V concentration, RF power and growth temperature on resistivity, transmittance and crystallinity were investigated. For the polymer substrates, both a high …

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Viscoelastic characterization of high concentration …

In the above expressions, ∆f n and ∆D n represent the measured changes when the crystal is loaded with both the film and high concentration protein solution while ... Viscoelastic properties of thin films probed with a quartz-crystal resonator. Phys Rev B, 46 (1992), pp. 7808-7815. View in Scopus Google Scholar. 21.

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Water‐Induced Phase Separation Forming Macrostructured Epitaxial Quartz

Noteworthy, only samples with a concentration of 1 mmol of Sr2+ (Sr/Si molar ratio of 0.06) within the amorphous silica matrix have the right quantity and homogeneous dispersion of salt to permit further crystallization into a …

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Demonstrating a Quartz Crystal Microbalance with …

Figure 3. (a) SEM image of the dried siderite layer on Au-coated quartz. The film peeled off in a corner, which allows an estimate of its thickness. ... and c 0∞ is the …

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and wetting films: electrostatic and steric stabilization

In the case of F108 films, the comparison of films and wetting films on quartz indicates film stability that is either electrostatic or steric in origin. On the basis of the effect of electrolyte concentration on film thickness, the transition from electrostatic to steric stabilization is demonstrated for both kinds of films.

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Wettability of quartz in presence of nonionic surfactants and …

The addition of a short chain alcohol to aqueous solutions of nonionic surfactants (Triton X-100 and Triton X-165) independently on their constant concentration causes the increase of quartz wettability (Fig. 1a, Fig. 1b, Fig. 1c, Fig. 2a, Fig. 2b, Fig. 2c).The biggest changes of quartz wettability were observed in the range of alcohol …

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Layer‐by‐Layer Construction of Hybrid Film Based on PEI …

The concentration of NH 4 P 5 W 30 POM dipping solution is taken as 5 mM for improved adsorption. ... Formation of Multilayer Film on Gold Quartz Electrode. The gold crystal electrodes were modified using the same technique used to create multilayer films on gold electrodes. After cleaning the gold quartz electrodes, the electrode was …

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Rapid Detection of ppt Concentration of Perfluorooctane …

Abstract Identifying trace levels of perfluorooctane sulfonate (PFOS) at parts per trillion (ppt) in water remains a formidable task. Here, we fabricated MOF-808 through rapid microwave synthesis. Characterization of the synthesized MOF-808 involved techniques including XRD, FT-IR, SEM, and nitrogen sorption analysis. We integrated …

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Measurements of liquid film thickness, concentration, and …

A multi-wavelength near-infrared (NIR) diode laser absorption sensor has been developed and demonstrated for real-time monitoring of the thickness, solute concentration, and temperature of thin films of urea–water solutions. The sensor monitors the transmittance of three near-infrared diode lasers through the thin liquid film. Film …

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Growth and Crystallization of SiO2/GeO2 Thin Films on …

The growth of α-quartz-based piezoelectric thin films opens the door to higher-frequency electromechanical devices than those available through top-down approaches.We report on the growth of SiO 2 /GeO 2 thin films by pulsed laser deposition and their subsequent crystallization. By introducing a devitrifying agent uniformly within …

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Preparation and Photodegradation of TiO 2 Thin Films on …

The title of this article emphasizes that the TiO 2 film grows inside the quartz tube, but this part is not mentioned in the introduction. 3. The figure of the photocatalytic degradation mechanism has no figure caption. ... Line 92 "However, when the TBT concentration reached 10%, the growth rate of the TiO2 films decreased …

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A Review of Quartz Crystal Microbalance for Chemical and …

Short exposure to large amounts of PCP could be fatal. A concentration of 0.526 µM of PCP solution in an L-15 serum-free media was used to investigate water …

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Quartz crystal microbalances (QCM) are suitable …

Quartz crystal microbalance (QCM) A QCM consists of a piezo-electrically driven quartz crystal which is kept vibrating at its resonance frequency (eigenfrequency) by an electric feedback …

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Palladium and platinum thin films for low-concentration …

In this study, palladium (Pd) and platinum (Pt) thin films are prepared via RF sputtering method with approximately 2 nm thicknesses on quartz substrates. Temperature-dependent resistances of Pd and Pt thin films are investigated at a temperature range from 30 to 130 °C. The results show that the resistance is directly proportional to temperature. …

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Interpretation of the adsorption of metals on quartz crystal …

Before film deposition, the porphyrin compound was dissolved in chloroform resulting in a solution of concentration equal to 2.9 10 –2 mol L −1. Then, the gold …

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Preparation and Photodegradation of TiO2 Thin Films on the …

Titanium dioxide thin films on the inner wall of quartz tubes were prepared in situ by the sol–gel method. Meanwhile, copper and cerium were loaded onto the surface of the titanium dioxide thin films to enhance photocatalytic activity and broaden the range of light absorption. X-ray diffractometer, X-ray photoelectron spectroscopy, scanning electron …

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Quartz crystal microbalances (QCM) are suitable for real …

Quartz crystal microbalances (QCM) are suitable for real-time dosimetry in nanotoxicological studies using VITROCELL®Cloud cell exposure systems ... (dynamic …

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(PDF) Quartz Films: Water-Induced Phase Separation Forming

Quartz Films: Water-Induced Phase Separation Forming Macrostructured Epitaxial Quartz Films on Silicon (Adv. Funct. Mater. 35/2014)

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A practical guide to quartz crystal microbalance …

Delamination often occurs due to mechanical mismatch between the polymer film and the quartz crystal caused by large changes in the external environment, such as humidity, temperature, and pH. ... At …

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Thin liquid films from polyoxyethylene-polyoxypropylene …

The experimental cell [21] for film thickness measurements is shown in Fig. 1.It is similar to the cell described in our previous work [22], however the film is observed through the transparent solid substrate (fused quartz).The Teflon cell 1 was filled with the investigated solution 2. The fused quartz plate 3 was installed on the bottom of the cell.

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Protein film formation on cell culture surfaces investigated …

Quartz crystal microbalance with dissipation monitoring (QCM-D) was used to study the protein deposition kinetics and the mechanical properties of the protein films. …

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Determination of chemical oxygen demand values by a …

Martyanov and Klabunde compared TiO 2 particles in powder form and as a thin nanostructured film on quartz [29]. As a result, the photocatalytic activity of TiO 2 on quartz was better than that in the powder form because of higher quantum yields. In this paper, a COD measurement by a photocatalytic oxidation method using nano-TiO 2 …

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